The Three Additions to Daniel, a Study

to it. At first this is not apparent, since it remains colourless in the solution; but after a time, after floating a few sheets of paper, the organic silver compound gra

r washed cotton-wool, when it will be found decolourized. Another mode of getting the liquid out of the bottle is to syphon it off by any syphon arrangement, and this prevents a waste in the solution from the absorption of the filtering medium. The accompanying arrangement (fig. 4) will be found useful for the purpose, and can be applied to other solutions where decantation is necessary. A is a wide-mouthed bottle holding

g.

g.

ht part of the flame in the position shown; by this means a good length of it gets heated, and a

m the formation of nitric acid.[13] This must be neutralized unless a little silver carbonate is left at the bottom of the bottle as described at page 20. A camphor solution may also be added for the same purpose. Make a saturated soluti

rose tint. The theory is that the organic matter is oxidized by the oxygen liberated from the permanganate, and falls to the bottom

ith the oxidized organic matter will fall to the bottom. This plan answers admirably when time is no object, but in dull weather the action is slow. When once the precipitation fairly commences it goes on quickly, an

but it must be borne in mind that each sheet of paper floated on the solution trans

g.

with its contents, over a Bunsen burner or spirit lamp flame till it is red hot. The heat will destroy all organic matter, leaving a residue of carbonous matter behind, which, after subsequent operations, will be eliminated by filtration. Next cover the silver with nitric acid,[16] and in an evaporating dish slightly warm it over a spirit lamp or Bunsen burner. Red fumes will appear, and when all action has ceased, more acid must be added till such a time that very nearly (but not quite) all the silver is dissolved up. Then evaporate off all the fluid and allow it to cool, when water can be added to such an extent that it is over strength for the bath. Now measure the whole bulk of the solution in a glass measure, and test by the argentometer for strength. An argentometer is, in reality, an instrument for taking the specific gravity of a liquid. It is as shown in the figure. A B is a glass tube, inside of which is a graduated scale showing grains; C is a hollow glass cylinder, which has a little glass ball filled with mercury. When immersed in water, the instrument sinks till the scale reads 0